Specimen
Punch

Prepares high-quality disk specimens. A precision ground punch and
die plate eliminate specimen stress and distortion. For convenient
handling, a spring loaded return plunger keeps the disk specimen
on the die plate surface. The Specimen Punch is available in standard
sizes of 2.3 mm and 3.0 mm. Other sizes are available upon special
request
Model 220 Low-Temp Container
The
Low-Temp Container is designed for use with Model 110 Twin-Jet Electropolisher
for applications at cryogenic temperatures. Cooling is accomplished
via conduction from a cooling media such as liquid nitrogen and
methanol to the electrolyte contained in a glass dish. The dish
is supported in the Low-Temp Container while being surrounded by
the cooling media. Double wall, heavily insulated construction maintains
temperature during the electropolishing process. For temperature
monitoring, a hole is provided in the top plate for easy thermometer
access. The one-piece Low-Temp Container is manufactured entirely
from electrolyte resistant materials.
Model 140 Digital Power Control
The
Model 140 is specifically designed for use with the Model 110 Twin-jet
Electropolisher for electrolytic polishing or etching of specimens
for Transmission Electron Microscopy. It controls the electrolyte
flow, polishing voltage and current, the light source and photocell
shutoff circuit, and includes visual and audible alarms. Digital
displays allow for precise setting and reading of the electropolishing
voltage and current levels. The voltage can be varied between 0
and 120 volts, while the polishing current range is 0 and 100 mA.
The selectable mode feature of the Model 140 provides
the user with a high degree of flexibility. Two independent 3 position
switches, one for the Pump Select and one for the Polish Select
determine the mode of operation. The function of both switches is
to enable or inhibit the photocell shutoff circuitry.
With the Pump Select switch in the Auto mode,
the photocell circuitry immediately stops the electrolyte flow at
the first sign of light penetration through the specimen. In similar
fashion, the Polish Select switch stops the polishing current at
light penetration while in the Auto mode. With the Pump Select switch
in the Continuous mode, the pump remains activated after the light
has penetrated the specimen and the photocell circuitry has activated
the alarms. This feature allows the polishing time to be extended
past the point of a small perforation in the specimen.
The Polish Select switch is also used to control
the light source. In the Auto and Continuous modes, the light source
for the photocell circuit is illuminated. In the “Off”
position, both the light and the polishing current are off, allowing
for easy set-up of the Model 110 Electropolisher.
The photocell circuitry is designed to detect
the first sign of light penetration through the specimen. When this
occurs, independent of the position of the Pump and Polish Select
switch, both an audible and visual alarm are activated. A sensitivity
control adjusts the amount of light required to activate the photocell
shutoff. An Alarm Silent switch enables the audible alarm to be
silenced while the alarm light remains illuminated.
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